منابع مشابه
A simplified green approach for synthesis of arylquinoxalines under solvent-free clay-catalysed conditions
A friendly benign, green, rapid and facile strategy for synthesis a series of arylquinoxalines was achieved by condensation of aromatic 1,2-diamines with arylglyoxals under clay-catalyzed as an inexpensive and eco-friendly catalyst using grindstone chemistry. Significant decreases in reaction times and high yields have been observed by this green chemistry approach in comparison with previously...
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A green protocol has been applied to synthesize a novel series of 3-cyano-2-(tri-O-acetyl-β-D-arabinopyranosylthio)pyridines in a short reaction time, in higher yields and with simpler operations, when compared with the conventional heating method. Deacetylation of the obtained acetylated arabinosides produced 2-(β-D-arabinopyranosylthio)-3-cyanopyridines. The structures of the obtained product...
متن کاملNatural Acid Catalyzed Synthesis of Schiff Base under Solvent-free Condition: As a Green Approach
The reaction of primary aromatic amines with aryl aldehydes is found to be catalyzed by lemon juice as natural acid under solvent-free conditions to give the corresponding Schiff bases in good yields. This eco-friendly reaction has many advantages like economical, environmental, mild reaction conditions and simple work-up with high product yield.
متن کاملSolvent-Free Green and Efficient One-Pot Synthesis of Dihydropyrano[3,2-c]chromene Derivatives
A rapid, clean, and highly efficient method for synthesis of dihydropyrano[3,2-c]chromene derivatives by one-pot, three-component condensation of aromatic aldehydes, malononitrile, and 4-hydroxycoumarin using DABCO as catalyst in solvent-free neat conditions is described. The present method has the advantages of mild reaction conditions, short reaction times, easy isolation of products, and exc...
متن کاملGreen one pot solvent-free synthesis of pyrano[2,3-c]-pyrazoles and pyrazolo[1,5-a]pyrimidines.
Pyrano[2,3-c]pyrazoles are obtained via mixing ethyl acetoacetate, hydrazine hydrate, aldehydes or ketones and malononitrile in the absence of solvent. These same products were also obtained by reacting arylidenemalononitriles 3 with 3-methyl-2-pyrazolin-5-ones. NOE difference experiments confirmed that these products exist solely in the 2H form. Similar treatments of 3-amino-2-pyrazolin-5-one ...
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ژورنال
عنوان ژورنال: Química Nova
سال: 2015
ISSN: 0100-4042
DOI: 10.5935/0100-4042.20150080